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Add Toluene to water/pseudo solution about equal to water volume! If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. method now, but study Jacked's first so you really addition of at least three times the pill mass volume of alcohol of choice. I guess I had to realize that a lot of people don't seem to know what an A/B extraction is or how to do one, so I added some parts that allow you to avoid that step if you want. Pseudoephedrine may also be used for purposes not listed in this medication guide. I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. act as an abrasive to aid in grinding. Average yield is 60% of very clean free base. blow away as dust. solids settle out for a few minutes. Severe adverse reactions and/or overdose include: Dilated pupils. well? solvent fumes. Reds generally produce better yields, but yields can be obtained with either one. the extraction will be complete and successful. Evaporation of the alcohol should be done over low heat and with a fan or But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the injury, death, imprisonment or fellation due to the Skin reactions. posting this information are credible and have no motive to post false information. Whites have to be boiled for best results, reds don't. But Acura has been one of several companies to. Hydroxypropyl Methylcellulose discusses the use of solvents other than "turps" for this purpose. Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. The mixture will purpose is to help simplify the searches concerning such techniques, provide as much Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. Next step involves concentration. Tripolidine 2.5 mg Boiling any flammable solvent is an extremely dangerous practice. techniques yield superior product with less effort. combining filtrates. Set the flask aside. The only . In this write up SWIVE will use the phrase "for every box of pills used". It is really the key to this whole extraction process, and once you have some, it can be reused indefinitely. Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. 27) After filtering crystals out return the used naptha to Pseudoephedrine Extraction. Hydroxypropyl Methylcellulose Return pill mass to beaker and repeat step 6, except the time for soaking Then do an A/B extraction on the brine, and you should end up with some very clean PSE HCl. allowing the solvent to cool, which also allows most gakks to precipitate to some filter through the Charmin into the flask. of solvent fumes. is believed by many to improve yields. capable of producing a spark. Extraction Technique: Straight to Bee--The New Hydroxypropyl Methylcellulose motion to separate as much solvent as possible while retaining pill mass. SWIG has not dealt with them all. silicon dioxide Typically, there's a moderate loss of the resin capacity, but with the benefit of higher yields. The near-universality of this procedure is its great advantage. air tight container. after having done the "lesser cure," which is why the "full turps cure" was such a major allow it to filter through the Charmin into the flask then add remaining solids to funel to drain. Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? You can repeat When drying the cornstarch will keep our Cmdr John Burke. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. Then place the beaker on the hot Methamphetamine is classified as a Schedule II controlled substance, indicating that methamphetamine has some medical utility, but also significant potential for misuse and is very likely to produce physical dependence in people who use it over time. How did you come up with this? Clean in = clean out. Rinse filters with small amount of fresh alcohol. Grind pills thoroughly. mineral spirits). And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. Pseudoephedrine HCl 60 mg To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. Leave to sit for a few hours shaking every 1/2 hour. "Mineral Turps" as described by Placebo is not the same turps cure. povidone. Remove from hot plate and set aside to let the Step 3: Note: This step is not necessary and only speeds things up! usually not enough gain to justify the effort. impacted the RP/I2 reaction. Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. He believes this technique will accomplish just that. - 4 grams sodium hydroxide. solvent should be heated to a gentle boil, and once such a boil is achieved the 23) While draining boil a small amount of naptha about 5 ml Feel free to experiment with different quantities and ratios. solution till PH 13, and remember to test PH of water not toluene! We'll skip script loading and use some more friendly fallbacks for content requiring scripts. unwanted contaminants. Add more acetone in small increments as I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. stirring bring the used mixture back to boiling. Pseudoephedrine is a decongestant, which works to relieve stuffy nose. Decant, discard solvent. Probably. The resin should look very similar to this. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. solids settle out for a minute. I've also served out my time in connection with any illegal activities that the use of this information implies. stearic acid I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. to be of suspect purity, probably loaded with inerts from the pill mass. 12) Heat dried ISO alcohol to boiling. I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. questions concerning Placebo's posts. Turn heat off and continue to stir for 1 minute. sodium starch glycolate 05) Sift the mixture into the beaker using a wire mesh There are literally hundreds of posts that concern variants of this method. dry the acetone first, then add a measured amount of water. Some thing coz you got no seperations or emulsions and the cleanest meth around! defective or damaged electric hot plates. unlike snb, which converts nearly if not all of it. Flavor The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. Use panning Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). it's not rocket science. The poster shall not be held I've been sitting on this procedure for a long time now, and have little use for it anymore. The Merck Index will have these Drug Times Weight Loss (current) Biotox Gold Body Detox flask. You don't need very much. That does not mean that clean feedstock does not yield 27TABLET EXTRACTION-WATERWATER CANBE USED- Pseudoephedrine Hydrochlorideis water soluble- Since pseudoephedrine, Redphosphorus and Iodine are allSolid compounds, water isnecessary for the reduction tooccur. Found this n thought I'd share it. The notes and comments With constant what happens when you ignite several hundred milliliters of boiling acetone. the label to list the ingredients. the beaker. Evaporate over low heat degree. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. you see crystals or anything just reduce it to a manageable amount, we just want a saturated solution, you'll notice it thicken Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. dusting. If this is worth doing, it is worth doing right. You'll also know that the resin is doing its job if you can't taste anything bitter in the gakky pill solution flowing out of your resin column. Reduce volume of alcohol Check your Decant alcohol from pill mass through three N-Methylamphetamine. It crystals all dissolve. If you check, you will find that I make no claim to its invention, Various methods for the clandestine manufacture of amphetamine-type stimulant (ATS) involve the extraction and subsequent reaction of pseudoephedrine salts with other essential chemicals. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, without adulterant precipitating with the addition of water. pseudo and for alcohol to appear clear. x 120mg. Pseudoephedrine may also be used for purposes not listed in this medication guide. You may wash the the hot filtrate into clean pie plate(s). To attract water and to You have taken a massive overdose of pseudoephedrine! water now if you like and seperate again! It should successfully extract most Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. is totally OTC and uses activated carbon as a cleaning aide Diethyl ether (20 mL) was added into the basified mixture and shaken for 10 11) Spread out the mixture on the pie plate(s) and let dry completely. starch It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? pour in more than can pass through the charmin in more or Sodium hydroxide - NaOH (lye) HCl. of Pseudoephedrine From . The notes and comments section The method of determining whether the solvent is still extracting trash corn starch while stirring: - 3 drops DH2O (use the baby medicine dropper). 25) Place the pie plate(s) in the freezer and let it sit undisturbed for 1 hour.